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2004, (04)

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同仁大活络丹与同仁牛黄清心丸红外指纹图谱的研究
Studies on IR fingerprint of Tongren Dahuoluo pills and Tongren Niuhuangqingxin pills

田进国,张静,任健,胡爱平,高彦慧,娄红祥
TIAN Jin guo 1, ZHANG Jing 2 ,REN Jian 1, HU Ai ping 2 ,GAO Yian hui 1, LOU Hong xiang 1 (1. School of Pharmacy, Shandong University, Jinan 250012, China; 2. Beijing Tong Ren Tang Pharmaceutical Factory, Beijing 100011, China )

摘要(Abstract):

目的 :分别确定同仁大活络丹与同仁牛黄清心丸的红外指纹图谱。方法 :对大蜜丸剂采用统一的提取方法 ,对每一个样品都依次用正己烷、乙醚和丁酮提取并测试其提取物的红外指纹图谱。结果 :2 5批同仁大活络丹与 2 7批同仁牛黄清心丸的样品分别具有独特而稳定的红外指纹图谱。结论 :经过数据平均 ,同仁大活络丹与同仁牛黄清心丸的红外指纹图谱可以作为其质量控制和真伪鉴别的根据。
Objective: To identify Tongren Dahuoluo pills and Tongren Niuhuangqingxin pills respectively by analysis of IR fingerprint. Method: Both drugs were extracted with hexane, ethylether and butanone respectively and then the obtained extracts were measured with the FT-IR spectrometer. Result: By analyzing IR fingerprint of 25 batches of Tongren Dahuoluo pills and 27 batches of Tongren Niuhuangqingxin pills , we found that different batches of the same drug hadstabile and repeatable fingerprint. Conclusion: By using IR fingerprint , either Tongren Dahuoluo pills or Tongren Niuhuangqingxin pills can be exactly identified.It provides a rapid method for drug identification and quality control.

关键词(KeyWords): 同仁大活络丹;同仁牛黄清心丸;大蜜丸;红外指纹图谱
Tongren Dahuoluo pills; Tongren Niuhuangqingxin pills; big honeyed pills; IR fingerprint

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作者(Author): 田进国,张静,任健,胡爱平,高彦慧,娄红祥
TIAN Jin guo 1, ZHANG Jing 2 ,REN Jian 1, HU Ai ping 2 ,GAO Yian hui 1, LOU Hong xiang 1 (1. School of Pharmacy, Shandong University, Jinan 250012, China; 2. Beijing Tong Ren Tang Pharmaceutical Factory, Beijing 100011, China )

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