桃仁脂肪酸GC-MS指纹图谱研究GC-MS fingerprint analyses of fatty acids in peach seed
裴瑾;颜永刚;万德光;莫书蓉;
PEI Jin1*,YAN Yonggang2,WAN Deguang1,MO Shurong1(1.Chengdu University of Traditional Chmese Medicine,Chengdu 610075,China;2.Shanxi University of Chinese Madicine,Xianyang 712046,China)
摘要(Abstract):
目的:对桃仁脂肪酸进行气相色谱指纹图谱研究,为桃仁的质量评价提供依据。方法:利用毛细管气相色谱对桃仁脂肪酸进行分析,并利用GC-MS技术确认指纹图谱中的特征指纹信息,进行系统聚类和相似度分析。结果:对34批不同产地、品种的桃仁进行了测定,获得了较为理想的包含特征信息的桃仁GC指纹图谱。结论:本方法重复性好,所建立的指纹图谱为桃仁药材的质量控制提供了有效手段。
Objective: To investigate the GC fingerprint of fatty acids in peach seed,and provide evidences for quality assessment on peach seed.Method: Capillary gas chromatography was applied in analysis of fatty acids in peach seed,and the distinctive information was confirmed by GC-MS with hierarchical cluster and species similarity analysis.Result: The GC fingerprint containing distinctive information was obtained after investigation of peach seeds from 34 varieties and origins.Conclusion: With Good reproducibility,fingerprints established for peach seeds provided an effective method for quality control.
关键词(KeyWords):
桃仁;GC-MS;指纹图谱
peach seed;GC-MS;fingerprint
基金项目(Foundation): 四川省中医药管理局科研项目
作者(Author):
裴瑾;颜永刚;万德光;莫书蓉;
PEI Jin1*,YAN Yonggang2,WAN Deguang1,MO Shurong1(1.Chengdu University of Traditional Chmese Medicine,Chengdu 610075,China;2.Shanxi University of Chinese Madicine,Xianyang 712046,China)
Email:
DOI:
参考文献(References):
- [1]中国药典.一部[S].2005:196.
- [2]颜永刚,裴瑾,万德光.桃仁脂溶性成分GC-MS法分析[J].新疆大学学报:自然科学版,2007,24(增刊):221.
- [3]胡锐,李宝莉.多不饱和脂肪酸对心血管系统的作用及机制[J].西北药学杂志,2008,23(2):118.
- [4]刘荣霞,周婷婷,董婷霞,等.建立评价当归质量的HPLC指纹图谱分析方法[J].中国药学杂志,2003,38(10):757.
- [5]王玺,王文宇,张克荣,等.中药HPLC指纹图谱相似性研究的探讨[J].沈阳药科大学学报,2003,20(5):360.
- [6]林小明.桃仁化学成分和药理作用研究进展[J].蛇志,2007,19(2):130.
- [7]原田正敏.汉方生药と制剂の品质评价[M].东京:广川书店株式会社,1992:76.
- [8]颜永刚,裴瑾,万德光.HPLC法测定不同产地和品种桃仁中苦杏仁苷[J].中草药,2008,39(9):1415.
- [9]袁丹,胡爽,毕开顺,等.桃仁药材质量评价法的研究[J].中国药学杂志,2003,38(1):53.
- [10]王友兰,李红兵,华玉琴.HPLC法测定桃仁中苦杏仁苷的含量[J].中国药师,2002,5(9):555.
- 裴瑾
- 颜永刚
- 万德光
- 莫书蓉
PEI Jin1*- YAN Yonggang2
- WAN Deguang1
- MO Shurong1(1.Chengdu University of Traditional Chmese Medicine
- Chengdu 610075
- China
- 2.Shanxi University of Chinese Madicine
- Xianyang 712046
- China)
- 裴瑾
- 颜永刚
- 万德光
- 莫书蓉
PEI Jin1*- YAN Yonggang2
- WAN Deguang1
- MO Shurong1(1.Chengdu University of Traditional Chmese Medicine
- Chengdu 610075
- China
- 2.Shanxi University of Chinese Madicine
- Xianyang 712046
- China)